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Severe gas hazards are increasing in deep mining areas, and there exists an enormous traditional challenge for protected seam mining. In this work, we conducted a multifaceted investigation into the spatiotemporal effectiveness exerted by pressure unloading from a distant safeguarded stratum in concert with the application of gas extraction methodologies. The stress and displacement evolution in the protected coal seam (PCS) are analyzed by applying Flac3D, and then positives are verified by the measurement of coal seam deformation and investigation of the unloading boundary. The results show that diminution coefficient of 0.62, and record an expansive deformation rate of 5.83%. The opportune temporal window for effective gas drainage is discerned, with its time window spans from 58 to 67 days as the expanse between 350 and 400 m progresses at the working face. Continuous and effective gas extraction occurs when transverse cracks in the PCS reach an optimal state of pressure relief. The final cumulative gas extraction was 320,300 m with an extraction efficiency of 34.3%. A residual gas volume of 3.68 m/t and a residual gas pressure of 0.5 MPa reflect the efficient gas extraction.
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http://dx.doi.org/10.1021/acsomega.4c04796 | DOI Listing |
Anal Chem
September 2025
Department of Chemistry, Wuhan University, Wuhan 430072, China.
Three-dimensional printing (3DP) technology enables the flexible fabrication of integrated monolithic microextraction chips for high-throughput sample pretreatment. Meanwhile, the extraction performance of 3DP-based channels is largely limited by printer resolution and the commercially available printing materials. In this work, a 3DP array monolithic microextraction chip (AMC) was fabricated by integrating 26-array helical monolithic microextraction channels for sample pretreatment and 52-array gas valves for fluid control.
View Article and Find Full Text PDFRSC Adv
September 2025
Food and Drug Safety Research Center, Pharmaceutical Sciences Institute, Tabriz University of Medical Sciences Tabriz Iran.
This study focuses on developing an analytical method to efficiently extract and concentrate several adipate and phthalate plasticizers that can migrate from plastic packaging into various wound disinfectants. The study employed an approach that combined dispersive micro solid phase extraction with dispersive liquid-liquid microextraction using ZIF-4 as an adsorbent. The adsorbent was thoroughly characterized to understand its properties.
View Article and Find Full Text PDFThe aim of the present study was to assess the anti-inflammatory effect of hesperidin. The research was conducted by optimizing the hesperidin extraction process from citrus peel powder, followed by characterization and nutrition profiling of citrus peel hesperidin extract. Citrus peel was collected from the local market and dried in a hot air oven.
View Article and Find Full Text PDFLeg Med (Tokyo)
September 2025
Department of Analytical Chemistry, School of Pharmacy and Pharmaceutical Sciences, Hoshi University, 2-4-41, Ebara, Shinagawa-ku, Tokyo 142-8501, Japan.
This study investigated headspace solid-phase microextraction (HS-SPME)-gas chromatography (GS)/mass spectrometry as a low-complexity method for accurate measurement of blood alcohol concentration (BAC) changes in humans over time following alcohol consumption. The aim was to develop an analytical method that would require as small blood samples as possible-smaller than that required for the conventional method-thereby reducing the burden on the subject. Polyethylene glycol (PEG) was used as the fiber material for SPME, and a DB-WAX capillary column was used for GC.
View Article and Find Full Text PDFEnviron Sci Pollut Res Int
September 2025
Faculty of Environment and Resource Studies, Mahidol University, Salaya, Phutthamonthon, Nakhon Pathom, 73170, Thailand.
Soil washing with surfactants is a promising technique for remediating petroleum hydrocarbon-contaminated soils. This study evaluates a biosurfactant extracted from Eichhornia crassipes (water hyacinth), an abundant aquatic weed in Thailand, using ultrasound-assisted extraction for diesel-contaminated soil remediation. The biosurfactant extract (Extract WH) was characterized for its surface tension reduction, critical micelle concentration (CMC), emulsification capacity with diesel, and phytotoxicity.
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