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It has become a trend to precisely control the additive manufacturing process parameters within the high-density process window to obtain high-performance metal parts. However, there are few reports on this topic currently, leaving this research without sufficient references. This study took 316L austenitic stainless steel as a case study. In total, 36 groups of specimens were manufactured by Laser powder bed melting (LPBF), and then, two highly dense specimens were selected to study the variation in their microstructure and properties. The densities of the selected specimens, S1 (VED = 81 J/mm) and S2 (VED = 156.3 J/mm), are 99.68% and 99.99%, respectively. The results indicated that, compared with the S1 specimen, the S2 specimen significantly decreased in terms of yield strength (YS), ultimate tensile strength (UTS), and elongation (EL), which are 7.28%, 6.34%, and 19.15%, respectively. The differences in mechanical properties were primarily attributed to differences in their microstructures. Further, compared with the S1 specimen, the fitted ellipse aspect ratio and average grain size of the S2 specimen increased by 79.88% and 53.45%, respectively, and the kernel average misorientation (KAM) value and geometric necessary dislocation (GND) density increased by 36.00% and 58.43%, respectively. Furthermore, the S1 specimen exhibited a strong texture in the <101>//Z direction, whereas no obvious texture was observed in the S2 specimen. Obviously, the reason why precise regulation within the dense parameter range can achieve better performance is that the microstructure and mechanical properties of the specimens prepared within the dense range are different. More importantly, this study provides a feasible framework for optimizing alloys with broad and dense parameter ranges, demonstrating the potential to achieve high-performance components through precise parameter control. Furthermore, the results reveal that even within a wide range of high-density forming parameters, significant variations in microstructure and mechanical properties can arise depending on the selected parameter combinations. These findings underscore the critical importance of meticulous process parameter optimization and microstructural regulation in tailoring material properties.
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http://dx.doi.org/10.3390/ma18163899 | DOI Listing |
Phys Chem Chem Phys
September 2025
Department of Physics, Mizoram University, Aizawl-796004, India,.
It is anticipated that wide-bandgap semiconductors (WBGSs) would be useful materials for energy production and storage. A well-synthesized, yet scarcely explored, diamond-like quaternary semiconductor LiZnGeS has been considered for this work. Herein, we have employed two well-known functionals GGA and mGGA within a framework of density functional theory (DFT).
View Article and Find Full Text PDFNanoscale
September 2025
College of Physics, Hebei Normal University, Shijiazhuang 050024, China.
MoSe nanosheet/Si heterojunction photodetectors were fabricated by a mechanical exfoliation method, and their electrical and optical properties at different temperatures were investigated. It was found that the MoSe nanosheet/Si heterojunction device exhibited excellent rectification characteristics at room temperature, and the rectification ratio gradually decreased with the decrease of temperature. The temperature-dependent electrical properties of the MoSe/Si heterojunction device were actually caused by the inhomogeneity of the potential barrier.
View Article and Find Full Text PDFInorg Chem
September 2025
Malta-Consolider Team and Department of Analytical and Physical Chemistry, University of Oviedo, Oviedo E-33006, Spain.
Hydrated magnesium sulfates (MgSO·HO) are known to form multiple hydration states ( = 0-11) and are essential in planetary science and thermochemical energy storage. Despite their significance in detecting extraterrestrial water reservoirs or in mineral (de)hydration cycles, it is still necessary to understand how the structure-property relationships of these materials evolve at different hydration levels when pressure is applied. Through a systematic first-principles computational investigation, we elucidate the key structural factors governing the densification mechanism under hydrostatic pressure of MgSO·HO crystals.
View Article and Find Full Text PDFLab Chip
September 2025
Department of Engineering Design, Indian Institute of Technology Madras, India.
Microfluidic devices offer more accurate fluid flow control and lower reagent use for uniform nanoparticle synthesis than batch synthesis. Here, we propose a microfluidic device that synthesizes uniform iron oxide nanoparticles (IONPs) for highly efficient intracellular delivery. The 3D-printed device was fabricated, comprising two inlets in the T-shaped channel with an inner diameter of 2 mm, followed by a helical mixing channel with a single outlet.
View Article and Find Full Text PDFLangmuir
September 2025
Institute of Technology for Carbon Neutralization, Yangzhou University, Yangzhou 225127, Jiangsu, China.
To expand the application scope of carbon steel, imparting superhydrophobicity to its surface offers an effective strategy to overcome its inherently poor corrosion resistance. However, in marine environments, conventional superhydrophobic coatings often suffer from limited mechanical durability and inadequate long-term corrosion protection. In this study, a durable superhydrophobic bilayer coating composed of PDMS-MWCNTs (top layer) and PDMS (bottom layer) was developed to address these challenges.
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