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Aim: The objective of this study was to evaluate the bond strength of universal adhesive systems in self-etch and etch-and-rinse modes at the repair interface between aged and new composite resins.
Materials And Methods: Composite resin (Filtek Z250) was thermocycled to represent aged composite resin to be repaired. New composite resin was placed over the aged substrate after surface conditioning: NC (negative control, no surface treatment), A (adhesive only), SBM (Scotchbond Multi-Purpose in etch-and-rinse mode), CSE (Clearfil SE Bond in self-etch mode), SBU (Single Bond Universal), ABU (All Bond Universal), and TBU (Tetric N-Bond Universal). Universal adhesives (SBU, ABU, and TBU) were applied both in etch-and-rinse and self-etch modes. 1 mm × 1 mm × 8 mm beams were sectioned, and microtensile bond strength was measured after 24 hours of water storage and 10,000 thermocycling processes ( = 20/group). The fracture surfaces were observed with a scanning electron microscope to evaluate the failure pattern.
Results: The repair bond strength between the old and new composite resins was material-dependent. Universal adhesives significantly improved the repair bond strength ( < 0.05), while no significant difference was observed between the etch modes (self-etch or etch-and-rinse) for each universal adhesive ( > 0.05). Thermocycling significantly reduced the bond strength in all groups ( < 0.05).
Conclusion: Universal adhesives in both etch-and-rinse and self-etch modes outperformed the conventional 3-step etch-and-rinse and 2-step self-etch adhesive systems in terms of resin repair bond strength.
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http://dx.doi.org/10.1155/2022/7663490 | DOI Listing |
Dent Mater J
September 2025
Department of Operative Dentistry, Nihon University School of Dentistry.
This study aimed to determine the influence of air abrasion on the shear bond strength (SBS) of universal adhesives when using different abrasive powders. The AquaCare Twin served as the injection device. The prepared bovine dentin specimens were air- abraded with alumina particles or bioactive glass before applying the universal adhesive (All Bond Universal, Clearfil Universal Bond Quick ER, or Scotchbond Universal Plus Adhesive).
View Article and Find Full Text PDFLangmuir
September 2025
Biophysical Chemistry Laboratory, Physical Chemistry Section, Department of Chemistry, Jadavpur University, Raja S. C. Mullick Road, Jadavpur, Kolkata 700032, India.
Photophysical studies on the interaction of small molecules with various forms of nucleic acids are attracting attention nowadays in order to delineate the molecular level mechanism of various biological processes occurring in vivo. Herein, we employed vivid steady-state and time-resolved spectroscopic techniques to elucidate the detailed characterization of the binding interaction of a biologically active cationic dye thioflavin T (ThT) with double and triple helical forms of RNA - A.U duplex and U.
View Article and Find Full Text PDFCarbohydr Polym
November 2025
College of Safety and Environmental Engineering, Shandong University of Science and Technology, Qingdao 266590, China; State Key Laboratory of Mining Disaster Prevention and Control Co-founded by Shandong Province and the Ministry of Science and Technology, Shandong University of Science and Technol
Aiming at the problems such as large dust in each production process of open-pit mines, insufficient water resistance of the curing layer of dust control materials, and poor mechanical strength, this research applied the network generated by Schiff base reaction between oxidized starch (OS) and gelatin (GEL) as the basis, and combined with polyvinyl alcohol (PVA) and calcium chloride (CaCl). This material improves the problem of poor dust suppression effect caused by the environment of open-pit coal mines. It was found that the large number of amino groups contained in GEL attack the carbon atoms in the carbonyl group of OS to form carbon-nitrogen double bonds, generating Schiff bases as the crosslinking network, which enhanced the water resistance of the polymers.
View Article and Find Full Text PDFJ Prosthodont
September 2025
Department of Prosthodontics, Faculty of Dentistry, Ataturk University, Erzurum, Turkey.
Purpose: Debonding of zirconia restorations remains a significant clinical challenge due to its glass-free microstructure, which limits micromechanical and chemical adhesion. Zircos-E, a nitric-hydrofluoric acid mixture, has been proposed as a simplified room-temperature alternative to airborne-particle abrasion (APA). This meta-analysis aimed to compare the shear bond strength (SBS) of zirconia surfaces treated with Zircos-E etching versus APA.
View Article and Find Full Text PDFChem Sci
August 2025
College of Polymer Science and Engineering, State Key Laboratory of Advanced Polymer Materials, Sichuan University Chengdu 610065 China
Polyphenol-derived vitrimers offer compelling prospects for sustainable materials owing to their intrinsic recyclability, reprocessability and biodegradability. However, practical development remains constrained by structure degradation under harsh reprocessing conditions and the need for sophisticated modifications of the bio-sourced precursors. Herein, we reported a strategy that integrates commercially available polyphenols and low-molecular-weight PDMS through adaptable iminoboronate chemistry, obviating the need for structural modifications.
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