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Unlabelled: Development of new materials for tooth bleaching justifies the need for studies to evaluate the changes in the enamel surface caused by different bleaching protocols.
Objective: The aim of this study was to evaluate the bovine dental enamel wear in function of different bleaching gel protocols, acid etching and pH variation.
Material And Methods: Sixty fragments of bovine teeth were cut, obtaining a control and test areas. In the test area, one half received etching followed by a bleaching gel application, and the other half, only the bleaching gel. The fragments were randomly divided into six groups (n=10), each one received one bleaching session with five hydrogen peroxide gel applications of 8 min, activated with hybrid light, diode laser/blue LED (HL) or diode laser/violet LED (VHL) (experimental): Control (C); 35% Total Blanc Office (TBO35HL); 35% Lase Peroxide Sensy (LPS35HL); 25% Lase Peroxide Sensy II (LPS25HL); 15% Lase Peroxide Lite (LPL15HL); and 10% hydrogen peroxide (experimental) (EXP10VHL). pH values were determined by a pHmeter at the initial and final time periods. Specimens were stored, subjected to simulated brushing cycles, and the superficial wear was determined (μm). ANOVA and Tukey´s tests were applied (α=0.05).
Results: The pH showed a slight decrease, except for Group LPL15HL. Group LPS25HL showed the highest degree of wear, with and without etching.
Conclusion: There was a decrease from the initial to the final pH. Different bleaching gels were able to increase the surface wear values after simulated brushing. Acid etching before bleaching increased surface wear values in all groups.
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http://dx.doi.org/10.1590/1678-775720150281 | DOI Listing |
Mikrochim Acta
September 2025
Affordable and Sustainable Sample Preparation (AS2P) Research Group, Departamento de Química Analítica, Instituto Químico para la Energía y el Medioambiente IQUEMA, Universidad de Córdoba, Campus Universitario de Rabanales, Edificio Marie Curie, E-14071, Córdoba, Spain.
Stainless-steel substrates have grown in importance in the development of planar sorptive phases. However, the reduced wettability of polished sheets makes difficult their functionalization. This limitation can be solved by using amorphous silica gel microparticles as superficial guides.
View Article and Find Full Text PDFACS Appl Mater Interfaces
September 2025
State Key Laboratory of Fluid Power and Mechatronic Systems, Zhejiang University, Hangzhou, Zhejiang 310058, China.
We report an electro-enhanced catalytic etching approach for direct atomic-level patterning of single-crystal 4H-SiC (0001) surfaces. The process utilizes platinum-coated probes under a negative sample bias, which enhances catalytic reactions and promotes etching of SiC without additional mechanical load. Unlike traditional etching approaches that rely on hazardous chemicals such as hydrofluoric acid, this approach operates under ambient conditions, offering improved safety and environmental compatibility.
View Article and Find Full Text PDFACS Omega
September 2025
National Key Laboratory of Oil and Gas Reservoir Geology and Exploitation, Southwest Petroleum University, Chengdu, Sichuan 610500, China.
Conventional acidizing struggles to remove complex, organic-rich scales in oil wells, and while strong organic solvents can help, their high cost and safety risks limit field use. To overcome these shortcomings, we developed a low-cost, safe permeability-enhanced-dispersion (PD) technique that first loosens and disperses the scale and then applies acid for thorough cleanup. The PD fluid (DL) contains a mutually soluble fatty alcohol amide phosphate dispersant (DL-F), ethanol, a surfactant blend, and a self-generating acid.
View Article and Find Full Text PDFACS Appl Mater Interfaces
September 2025
Oil Crops Research Institute, Hubei Key Laboratory of Lipid Chemistry and Nutrition, Hubei Hongshan Laboratory, Key Laboratory of Oilseeds Processing, Ministry of Agriculture, Chinese Academy of Agricultural Sciences, Wuhan 430062, China.
This study reports the synthesis of bifunctional hollow double-layered mesoporous silica (HdlMS) nanoparticles as an effective support for enzyme catalysis. Using a self-template method combined with sol-gel processing, selective etching, and surface modification with alkyl groups and nitrogenous fatty amine groups, we successfully prepared the NH/C-HdlMS carrier. Phospholipase A1 was then immobilized onto this carrier to construct PLA1@NH/C-HdlMS, which was subsequently applied to the synthesis of docosahexaenoic-acid-enriched phosphatidylcholine.
View Article and Find Full Text PDFJ Prosthodont
September 2025
Department of Prosthodontics, Faculty of Dentistry, Ataturk University, Erzurum, Turkey.
Purpose: Debonding of zirconia restorations remains a significant clinical challenge due to its glass-free microstructure, which limits micromechanical and chemical adhesion. Zircos-E, a nitric-hydrofluoric acid mixture, has been proposed as a simplified room-temperature alternative to airborne-particle abrasion (APA). This meta-analysis aimed to compare the shear bond strength (SBS) of zirconia surfaces treated with Zircos-E etching versus APA.
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