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To prolong the service life of asphalt pavement and reduce its maintenance cost, a fiber Bragg grating (FBG) sensor encapsulated in carboxylated carbon nanotube (CNT-COOH)-modified gel material suitable for strain monitoring of asphalt pavement was developed. Through tensile and bending tests, the effects of carboxylated carbon nanotubes on the mechanical properties of gel materials under different dosages were evaluated and the optimal dosage of carbon nanotubes was determined. Infrared spectrometer and scanning electron microscopy were used to compare and analyze the infrared spectra and microstructure of carbon nanotubes before and after carboxyl functionalization and modified gel materials. The results show that the incorporation of CNTs-COOH increased the tensile strength, elongation at break, and tensile modulus of the gel material by 36.2%, 47%, and 17.2%, respectively, and increased the flexural strength, flexural modulus, and flexural strain by 89.7%, 7.5%, and 63.8%, respectively. Through infrared spectrum analysis, it was determined that carboxyl (COOH) and hydroxyl (OH) were successfully introduced on the surface of carbon nanotubes. By analyzing the microstructure, it can be seen that the carboxyl functionalization of CNTs improved the agglomeration of carbon nanotubes. The tensile section of the modified gel material is rougher than that of the pure epoxy resin, showing obvious plastic deformation, and the toughness is improved. According to the data from the calibration experiment, the strain and temperature sensitivity coefficients of the packaged sensor are 1.9864 pm/μm and 0.0383 nm/°C, respectively, which are 1.63 times and 3.61 times higher than those of the bare fiber grating. The results of an applicability study show that the internal structure strain of asphalt rutting specimen changed linearly with the external static load, and the fitting sensitivity is 0.0286 με/N. Combined with ANSYS finite element analysis, it is verified that the simulation analysis results are close to the measured data, which verifies the effectiveness and monitoring accuracy of the sensor. The dynamic load test results reflect the internal strain change trend of asphalt mixture under external rutting load, confirming that the encapsulated FBG sensor is suitable for the long-term monitoring of asphalt pavement strain.
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http://dx.doi.org/10.3390/gels11080590 | DOI Listing |
Mikrochim Acta
September 2025
National Research and Development Institute for Chemistry and Petrochemistry ICECHIM, 202 Splaiul Independentei Street, 060021, Bucharest, Romania.
Molecular recognition and determination of vascular cell adhesion molecule-1 (VCAM-1), interleukin-6 (IL-6), and natriuretic peptide C-type (NPPC) are essential for the early prognosis and diagnosis of cardiovascular diseases, especially in young obese populations. Highly sensitive and selective devices characterized by low Limits of quantification are required for their determination in whole blood. Therefore, a 3D stochastic sensor was developed by immobilizing a chitosan hydrogel onto a carbon paste electrode (used as the support matrix for the hydrogel), which was subsequently modified with gold nanoparticles, multi-walled carbon nanotubes, and β-cyclodextrin (β-CD/AuNPs@MWCNT/CS/CPE).
View Article and Find Full Text PDFCarbohydr Polym
November 2025
School of Materials Science and Engineering, Dongguan University of Technology, Dongguan 523808, China. Electronic address:
Aerogels are widely used in environmental remediation, but their application is hindered by brittleness, limited oil absorption and poor separation of viscous crude oil. In this study, a multifunctional superhydrophobic aerogel with electrothermal and photothermal effects was prepared from bacterial cellulose (BC), methyltrimethoxysilane (MTMS), and hydroxylated carbon nanotubes (HCNT) by soft-hard synergistic and directed freezing. The prepared aerogel exhibited an oriented layered porous structure with excellent compressibility and oil retention capacity.
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November 2025
Department of Chemistry, The Chinese University of Hong Kong, Shatin, N.T. 999077, Hong Kong. Electronic address:
The increasing global demand for food and the adverse environmental impacts of excessive agrochemical use highlights the urgent need for sustainable and scalable seed treatment technologies. This paper reports a novel photothermal seed coating (QC@SCCNTs) with high biocompatibility, exceptional photothermal efficiency, and notable reusability, serving as an effective alternative to conventional chemical treatments. The coating consists of sericin-functionalized carboxylated carbon nanotubes (SCCNTs) electrostatically complexed with quaternary ammonium chitosan (QC), forming a composite film (QS film).
View Article and Find Full Text PDFSmall
September 2025
Centre for Interdisciplinary Research, D. Y. Patil Education Society (Deemed to be University), Kolhapur, Maharashtra, 416 006, India.
Developing efficient, sustainable, earth-abundant, cost-effective electrocatalysts is extremely challenging. Cobalt-iron-layered double hydroxide nanosheets (Co-Fe-LDH NSs) hybridized with carbon nanotubes (CNTs) lead to anchors Co-Fe-LDH-CNTs (CFC) self-assembly with a mesoporous morphology, expanded surface area, fast charge transfer kinetics, and high electrical conductivity. The resultant anchored CFC nanohybrid is highly active for electrocatalytic oxygen evolution reaction (OER), showing a lower overpotential of 221 and 313 mV at a current density of 10 and 25 mA cm, respectively, compared to pristine Co-Fe-LDH (339 and 391 mV), showcasing the significant role of CNTs in improving the electrocatalytic performance of pristine Co-Fe-LDH.
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September 2025
Department of Mechanical Engineering, The Hong Kong Polytechnic University, Hong Kong, 999077, China.
Droplet electricity generators (DEGs) that generate electricity through the interplay between water and the dielectric materials have attracted growing research interest due to their remarkable output voltage. However, conventional DEG design faces a critical trade-off: regulating the properties of dielectric materials, such as thickness or permittivity, can enhance output voltage yet weaken transferred charge. Here, a fluorinated ethylene propylene (FEP)/multi-walled carbon nanotubes (MWCNTs)/polydimethylsiloxane (PDMS) composite-based droplet electricity generator (FMP-DEG) is presented to overcome the voltage-charge trade-off and thus achieve an enhanced energy conversion efficiency of 4.
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