98%
921
2 minutes
20
Dark-field (DF) imaging is a recent X-ray imaging modality which is promising because it gives access to information not resolved in conventional transmission X-ray imaging. The DF technique was first introduced as a loss of visibility of the grating interferometry modulations. DF signal is now measured with all the different X-ray phase contrast setups such as beam tracking or modulation-based imaging. Using a dedicated setup [Magnin (2023). , 5839-5842], we present in the present article combined measurements of small-angle X-ray scattering and DF signal on the same material. We confirm that DF imaging is sensitive to multiple refraction from a sample, as can be found in the literature on lung imaging, but we show that the DF signal is also sensitive to scattering events. Finally, we measure a porous membrane that creates both types of signal (scattering and refraction), showing that, contrary to existing models, it is difficult to be quantitative about DF.
Download full-text PDF |
Source |
---|---|
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC12321030 | PMC |
http://dx.doi.org/10.1107/S1600576725004017 | DOI Listing |
ACS Appl Mater Interfaces
September 2025
State Key Laboratory of Fluid Power and Mechatronic Systems, Zhejiang University, Hangzhou, Zhejiang 310058, China.
We report an electro-enhanced catalytic etching approach for direct atomic-level patterning of single-crystal 4H-SiC (0001) surfaces. The process utilizes platinum-coated probes under a negative sample bias, which enhances catalytic reactions and promotes etching of SiC without additional mechanical load. Unlike traditional etching approaches that rely on hazardous chemicals such as hydrofluoric acid, this approach operates under ambient conditions, offering improved safety and environmental compatibility.
View Article and Find Full Text PDFCureus
September 2025
Department of Urology, Gunma University School of Medicine, Maebashi, JPN.
Syphilis cases are increasing in Japan, highlighting the urgent need for rapid and accurate diagnosis. In primary syphilis, serological tests may yield negative results, so direct microscopic observation of remains an important but often underused diagnostic method. We present a simple, widely accessible phase-contrast microscopy system, featuring a USB camera and monitor, enabling high-clarity, real-time observation of live wild-type treponemes directly from patient lesions.
View Article and Find Full Text PDFJ Am Chem Soc
September 2025
Hunan Joint International Research Center for Carbon Dioxide Resource Utilization, School of Physics, Central South University, Changsha, Hunan 410083, China.
Single-atom Ni catalysts hold great promise for the acidic CO reduction reaction (CORR), owing to their high CO selectivity. However, their performance under industrially relevant high current conditions is limited by the weak interaction between isolated Ni-N sites and *COOH intermediates, restricting efficient CO conversion. Here, we introduced edge-rich Ni-N sites via support vacancy engineering to enhance *COOH adsorption, thereby boosting the CORR activity and selectivity in acidic media.
View Article and Find Full Text PDFACS Appl Mater Interfaces
September 2025
Department of Inorganic and Physical Chemistry, Indian Institute of Science, Bangalore 560012, India.
Fabrication of water-stable and atomically dispersed ruthenium catalysts for sustainable borrowing hydrogenation (BH) reactions is a long-standing challenge. Herein, we developed an atomically dispersed Ru catalyst that has been successfully employed for BH reactions in aqueous micelles under mild conditions. The micellar cooperativity with the hydrophobic knitted aryl polymers (KAPs) led to the formation of microconfinements, which act as the confined space for catalysis in water.
View Article and Find Full Text PDFCommun Mater
August 2025
Department of Physics, Technical University of Denmark, Lyngby, Denmark.
Dark Field X-ray Microscopy (DFXM) has advanced 3D non-destructive, high-resolution imaging of strain and orientation in crystalline materials, enabling the study of embedded structures in bulk. However, the photon-hungry nature of monochromatic DFXM limits its applicability for studying highly deformed or weakly crystalline structures, and constrains time-resolved studies in industrially relevant materials. Here, we present pink-beam DFXM (pDFXM) at the ID03 beamline of ESRF, achieving a 27-fold increase in diffracted intensity while maintaining 100 nm spatial resolution.
View Article and Find Full Text PDF