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The stability of the scanning unit in a scanning tunneling microscope (STM) is essential for achieving high-resolution imaging. In this study, we present a non-metallic STM with a mechanically isolated scanning unit, ensuring long-term drift stability, low backlash, and high repeatability. By decoupling the piezoelectric scanning tube (PST) from the piezoelectric motor tube (PMT), the design effectively minimizes motor-induced instabilities and vibrations, significantly improving STM performance. The use of non-metallic materials for key components prevents eddy current interference and ensures long-term reliability. A sapphire-based frame provides high stiffness and compactness, with an eigenfrequency of 16.2 kHz in bending mode, reducing vibration noise during atomic imaging. The system exhibits excellent stability, maintaining low drift rates in both the X-Y plane and Z direction, ensuring precise tip-sample alignment. The performance of the home-built STM was validated through high-resolution atomic imaging of graphite and TaS surfaces. The simple, compact, and high-precision stepping mechanism, along with its ability to operate at low voltage, reduces experimental complexity. These features facilitate advanced material studies in constrained environments, such as high magnetic fields and low temperatures.
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http://dx.doi.org/10.1016/j.ultramic.2025.114157 | DOI Listing |
Appl Radiat Isot
September 2025
Kahramanmaraş İstiklal University, Department of Energy Systems Engineering, Kahramanmaraş, Türkiye.
The rapid advancement of three-dimensional (3D) printing technologies has significantly expanded their potential applications such as sensors and detector technology. In this study, the gamma-ray shielding performance of ulexite-doped composite resins fabricated via Digital Light Processing (DLP) 3D printing was experimentally investigated to evaluate radiation attenuation capacity. Composite resins containing different ulexite loadings (0, 1, 3, and 5 wt%) were exposed to gamma rays at energies of 356, 662, 1173, and 1333 keV to evaluate their attenuation characteristics.
View Article and Find Full Text PDFBiol Trace Elem Res
September 2025
Department of Environmental Sciences, Faculty of Biological Sciences, Kohat University of Science and Technology Kohat, Khyber Pakhtunkhwa, 26000, Pakistan.
The aim of the study was to evaluate the toxic metals (TMs) pollution, bioaccumulation and its potential health risk via consumption of different vegetables irrigated by different water sources released from industrial estates of Khyber Pakhtunkhwa. Water (fresh and waste), soil and vegetables samples were collected in triplicates and acid digested. Digestion of samples were followed by evaporation and filtration and then assessed for TMs via atomic absorption spectrophotometer.
View Article and Find Full Text PDFChem Asian J
September 2025
Bio-Organic Division, Bhabha Atomic Research Centre, Mumbai, 400 085, India.
Fluorescent N-heterocyclic carbene (NHC) metal complexes are useful for various chemical and biological applications. In this study, we developed a simple strategy to synthesize BODIPY-linked NHC metal complexes involving Ag, Cu, Ni, and Pd. The synthesis began with the preparation of BODIPY-imidazolium salt as a precursor ligand.
View Article and Find Full Text PDFAngew Chem Int Ed Engl
September 2025
College of Chemistry, Zhengzhou University, 100 Kexue Street, Zhengzhou, 450001, China.
Achieving quantitative control over interlayer spacing in multilayer two-dimensional (2D) supramolecular organic frameworks (SOFs) remains a fundamental challenge. Here, we report a molecular pillar engineering strategy enabling programmable vertical expansion of bilayer architectures. By designing elongated bipyridine pillars L2/L3 (3.
View Article and Find Full Text PDFACS Appl Mater Interfaces
September 2025
State Key Laboratory of Fluid Power and Mechatronic Systems, Zhejiang University, Hangzhou, Zhejiang 310058, China.
We report an electro-enhanced catalytic etching approach for direct atomic-level patterning of single-crystal 4H-SiC (0001) surfaces. The process utilizes platinum-coated probes under a negative sample bias, which enhances catalytic reactions and promotes etching of SiC without additional mechanical load. Unlike traditional etching approaches that rely on hazardous chemicals such as hydrofluoric acid, this approach operates under ambient conditions, offering improved safety and environmental compatibility.
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