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With the continuous development of the diamond industry, the China-type cubic press (CCP) has gradually become larger. As a result, the volume of the tungsten carbide (WC) anvil has been increased. Considering that the WC anvil is sintered, a larger volume will deteriorate sintering quality, which could facilitate the formation of cracks during its operation. One feasible way to reduce the volume of the WC anvil is to decrease its diameter and height. Along these lines, in this work, by performing finite element simulations, it was found that a reduction in the diameter of the WC anvil would increase the von Mises stress (VMS) during the synthesis process, as well as reduce the service life of the WC anvil and the ultimate pressure of the CCP. At the same time, a smaller diameter of the WC anvil would cause a significant increase in the VMS of the base steel block, exceeding its yield limit. In addition, a reduction in the height of the WC anvil would lessen the VMS during the synthesis process, and the VMS of the base steel block will also decrease. A reduction in the height of the WC anvil will decrease the pretightening force on the WC anvil, thereby reducing its lateral support effect. When the interference fit was increased from 0.6 to 0.8 mm and the steel ring angle was changed from 1.5° to 1.1°, the pretightening force on the low WC anvil was similar to the pretightening force on the original WC anvil. Our work provides valuable insights for effectively reducing the volume of the WC anvil.
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http://dx.doi.org/10.1063/5.0217396 | DOI Listing |
J Phys Chem Lett
September 2025
Center for Science at Extreme Conditions (CSEC) and the School of Physics and Astronomy, The University of Edinburgh, EH9 3JZ Edinburgh, United Kingdom.
Through high-pressure diamond anvil cell experiments, we report the synthesis of two novel potassium superhydrides (KH-I and KH-II) and investigate their structural and vibrational properties via synchrotron X-ray powder diffraction and Raman spectroscopy, complemented by density functional theory (DFT) calculations. Above 17 GPa at room temperature, KH-II and H react to form KH-I; this reaction can be accelerated with temperature. KH-I possesses a face-centered-cubic () potassium sublattice with a slight rhombohedral distortion (space group 3̅).
View Article and Find Full Text PDFInt J Biol Macromol
September 2025
School of Physics, Aristotle University of Thessaloniki, 54124, Thessaloniki, Greece. Electronic address:
Keratins represent an important class of sulfur-rich structural proteins. In this study, the pressure response of α-keratin, extracted from sheep wool, was investigated using Raman spectroscopy up to 4 GPa. A non-polar liquid (a Fluorinert™ FC70/77 mixture) served as the Pressure Transmitting Medium (PTM) in a Diamond Anvil Cell (DAC).
View Article and Find Full Text PDFRev Sci Instrum
September 2025
State Key Laboratory of High Pressure and Superhard Materials, Jilin University, Changchun, China.
The diamond anvil cell is a powerful tool for investigating material behavior under extreme pressure and temperature, but achieving efficient and uniform heating remains challenging. This study introduces a ring-type furnace integrated into a gasket with a metal-insulator-metal sandwich structure, using tantalum (Ta) for heating, tungsten (W) for electrodes, and mica-ceramic powder for insulation, enabling stable and uniform heating up to 2000 K. A calibration method combining thermocouple data and finite element simulations ensures accurate temperature measurement.
View Article and Find Full Text PDFJ Am Chem Soc
September 2025
Material Physics and Technology at Extreme Conditions, Laboratory of Crystallography, University of Bayreuth, 95440 Bayreuth, Germany.
Polar metals have attracted growing interest due to both their significance in fundamental science and their potential functionalities. Here, we report the discovery of a novel polar metal, magnesium chloride MgCl, in which the metallicity of the polar structure is uniquely driven by attractive halogen interactions. MgCl was synthesized in laser-heated diamond anvil cells and observed at pressures of 28(2)-93(3) GPa.
View Article and Find Full Text PDFNat Commun
September 2025
Department of Physics, Washington University, St. Louis, MO, USA.
Pressure serves as a fundamental tuning parameter capable of drastically modifying all properties of matter. The advent of diamond anvil cells (DACs) has enabled a compact and tabletop platform for generating extreme pressure conditions in laboratory settings. However, the limited spatial dimensions and ultrahigh pressures within these environments present significant challenges for conventional spectroscopy techniques.
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