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Solid-state welding offers distinct advantages for joining reactive materials, such as magnesium (Mg) and its alloys. This study investigates the effect of linear friction welding (LFW) on the microstructure and mechanical properties of cast AZ91 (Mg-9Al-1Zn) and AZ91-2Ca alloys, which (to the best knowledge of the authors) has not been reported in the literature. Using the same set of LFW process parameters, similar alloy joints-namely, AZ91/AZ91 and AZ91-2Ca/AZ91-2Ca-were manufactured and found to exhibit integral bonding at the interface without defects, such as porosity, inclusions, and/or cracking. Microstructural examination of the AZ91/AZ91 joint revealed dissolution of the Al-rich second phase in the weld zone, while the Mn containing phases remained and were refined. In the AZ91-2Ca/AZ91-2Ca joint, the weld zone retained Ca- and Mn-rich phases, which were also refined due to the LFW process. In both joint types, extensive recrystallization occurred during LFW, as evidenced by the refinement of the grains from ~1000 µm in the base materials to roughly 2-6 µm in the weld zone. These microstructural changes in the AZ91/AZ91 and AZ91-2Ca/AZ91-2Ca joints increased the hardness in the weld zone by 32%. The use of digital image correlation for strain mapping along the sample gage length during tensile testing revealed that the local strains were about 50% lower in the weld zone relative to the AZ91 and AZ91-2Ca base materials. This points to the higher strength of the weld zone in the AZ91/AZ91 and AZ91-2Ca/AZ91-2Ca joints due to the fine grain size, second phase refinement, and strong basal texture. Final fracture during tensile loading of both joints occurred in the base materials.
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http://dx.doi.org/10.3390/ma14113130 | DOI Listing |
iScience
September 2025
State Key Laboratory of Advanced Marine Materials, Institute of Oceanology, Chinese Academy of Sciences, Qingdao 266071, China.
Super austenitic stainless steels (SASS) face challenges like galvanic corrosion and antibacterial performance when welded to carbon steel (Q235) in marine environments. This study demonstrates that adding 1.0 wt% cerium (Ce) to SASS refines the heat-affected zone (HAZ) grain structure (from 7 μm to 2 μm), suppresses detrimental σ-phase precipitation, and forms a dense oxide film.
View Article and Find Full Text PDFEur J Obstet Gynecol Reprod Biol
September 2025
GEPROMED, 4 Rue Kirschleger, 67000 Strasbourg, France; Department of Vascular Surgery, Kidney Transplantation and Innovation, University Hospital of Strasbourg, 1 Rue de la Prte de l'Hôpital, 67000 Strasbourg, France. Electronic address:
Objective: The objective of this study was to understand the behavior of explanted Essure® devices in humans, focusing on the atomic composition of the device in different areas.
Methods: We collected 50 explanted Essure® devices (Bayer, Switzerland), in 29 patients. The following systematic investigations were performed on each devices: eye-nacked and optical microscopy, X-ray Faxitron, spectral analysis, elemental analysis of the metallic structure to accurately define the metallic composition of the spire and correlate these findings with macroscopic and microscopic observations.
Ind Health
September 2025
School of Population Health, Curtin University, Australia.
This study aimed to provide information on exposure to welding fume in workplaces in Australia, and the use of control measures in these workplaces. Personal and static samples of welding fume particulates and gases were collected at 20 workplaces whilst welding was being undertaken. Study personnel also recorded observations of the workplace.
View Article and Find Full Text PDFMaterials (Basel)
August 2025
College of Mechanical and Electrical Engineering, Huangshan University, Huangshan 245041, China.
In this study, under varying PDSP (plunging depths of stirring pin) and process parameters, refill friction stir spot welding tests were performed on 6061-T6 aluminum alloy, relying on a stirring tool with a 12 mm sleeve diameter and an 8 mm stirring pin diameter. The results manifested the internal defects in the weld zone when PDSP was 0, notwithstanding the alterations in process parameters. However, these flaws disappeared when PDSP was 0.
View Article and Find Full Text PDFMaterials (Basel)
August 2025
Guangdong Foreweld Co., Ltd., Guangzhou 510300, China.
This study investigates the application of the Keyhole-Tungsten Inert Gas Welding (K-TIG) hot-wire filling welding technique with mechanical arc oscillation to weld a 95 mm-thick Ti-6Al-4V titanium alloy plate. The root layer thickness achieved with this technique reaches up to 17 mm, with an average filling thickness of 2.5 mm.
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