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Article Abstract
Recycling of sewage sludge and the endogenous phosphorus (P) is a promising strategy for sustainable development, while the disposal of heavy metals (HMs) in sewage sludge and the recovery of targeted P species remain challenges. An innovative method coupling electrokinetic treatment with pyrolysis was proposed in the present study to achieve the effective reclamation of available P and the separation of HMs from sewage sludge. The pristine and FeCl-assisted electrokinetic treatment were employed for the removal of HMs from sewage sludge and to modify the P species, and the subsequent pyrolysis (300-700 °C) was conducted for the recovery of available P along with the production of biochar. The X-ray absorption near-edge spectroscopy (XANES), P liquid nuclear magnetic resonance (NMR) spectroscopy, and sequential chemical extraction were used to systematically determine the evolution of P during the combined treatment of sewage sludge. 19.69-24.80 % of Ni, Cu, and Zn were removed from sewage sludge after pristine electrokinetic treatment, and the HM removal efficiency was further elevated to 47.01-56.86 % with the assistance of FeCl. Consequently, in comparison with the raw sewage sludge-derived biochars (SBs), the biochars derived from FeCl-assisted electrokinetic treated sewage sludge (FESBs) contained much lower HM contents and showed higher stability of HMs. The FeCl-assisted electrokinetic treatment converted alkaline biochars dominated by poorly soluble Ca-phosphates into neutral to slightly acidic biochars dominated by Al/Fe-associated phosphates. This transformation greatly improved the available P concentrations determined by diffusive gradients in thin film in FESBs by 0.6-1.3 folds compared to untreated SBs. Therefore, coupling FeCl-assisted electrokinetic treatment with pyrolysis could be a promising strategy to achieve the reclamation of available P and the separation of HMs from sewage sludge.
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| http://dx.doi.org/10.1016/j.jenvman.2025.125882 | DOI Listing |
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