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This work aimed to study the effect of defatting via the mixture of n-hexane and ethanol under different volume ratio on the changes of structural characteristics, functional properties and volatile compounds of Tenebrio molitor larvae protein (TMLP). The results showed that 1:0.6 vol ratio of n-hexane to ethanol rendered the highest defatting rate (P < 0.05), as well as led to the highest EAA/AA contents, sulfhydryl contents, surface hydrophobicity, solubility, water/oil holding capacities and emulsifying properties of TMLP (P < 0.05). However, higher volume ratio of n-hexane to ethanol led to negative impacts on functionalities of TMLP. Moreover, the contents of aldehydes and hydrocarbons which rendered off-flavour to TMLP significantly decreased with the increasing volume ratio of n-hexane to ethanol (P < 0.05), while the contents of pleasure flavour (hydrocarbons and ester compounds) were obviously enhanced. This study provides an eco-friendly defatting method on the processing of TMLP with superior quality attributes.
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http://dx.doi.org/10.1016/j.foodres.2024.114974 | DOI Listing |
Food Chem
September 2025
Chemical Engineering Department, Universidade Federal de Santa Maria, Av. Roraima, 1000-7, 97105-900 Santa Maria, Rio Grande do Sul, Brazil. Electronic address:
Green solvents offer promising alternatives to n-hexane for sustainable vegetable oil extraction. This study evaluated ethanol, isopropanol, acetone, and ethyl acetate for extracting oils from avocado pulp (AP), rice bran (RB), and soybean flakes (SF), focusing on oil quality and defatted meal properties. lnγ obtained by COSMO-SAC showed tendencies for effective interactions with solutes.
View Article and Find Full Text PDFFood Sci Biotechnol
September 2025
Department of Food Bioengineering, Jeju National University, 102 Jejudaehakno, Jeju, Republic of Korea.
Urban particulate matter (PM) significantly contributes to air pollution. was extracted using ethanol (SHE) and subsequently partitioned with n-hexane, chloroform, ethyl acetate, and water. Antioxidant activities of fractions, including DPPH and ABTS radical, hydrogen peroxide, hydroxyl radical scavenging activities, and metal chelating effects, were evaluated against oxidative damage induced by PM.
View Article and Find Full Text PDFChem Biodivers
August 2025
Chemical Research Division, Bangladesh Council of Scientific and Industrial Research, Dhaka, Bangladesh.
Ceriops decandra (Griff.) Ding Hou, a mangrove species (family: Rhizophoraceae), has been traditionally used for its medicinal properties. This study investigates the phytochemical composition along with antioxidant, antimicrobial, and antidiarrheal potentials of C.
View Article and Find Full Text PDFChirality
September 2025
Egyptian Drug Authority (EDA) formerly National Organization for Drug control and Research (NODCAR), Giza, Egypt.
The enantiomeric purity of Finerenone (FIN), a novel therapeutic for chronic kidney disease (CKD), is a critical quality attribute for ensuring patient safety. This study reports the first chiral HPLC method for the simultaneous determination of FIN and its enantiomer, developed and validated using a rigorous analytical quality by design (AQbD) framework. The method employs a CHIRALPAK AD-H column with an isocratic mobile phase of n-hexane: ethanol (62:38, v/v).
View Article and Find Full Text PDFCompr Rev Food Sci Food Saf
September 2025
School of Chemical Engineering, Sichuan University, Chengdu, China.
As an emerging green technique, liquefied petroleum gas (LPG) extraction demonstrates significant advantages for extracting natural lipophilic compounds, including high extraction efficiency, low-temperature operation, minimal solvent residue, easy solvent recovery, low energy consumption, environmental friendliness, and economic viability. This article systematically reviews the principles, equipment, key influencing factors, application cases, and comparisons with other extraction technologies, while also analyzing its safety, sustainability, and industrial potential. LPG (primarily composed of propane and butane) enables efficient extraction under mild pressure (0.
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