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The adoption of green technology is very important to protect the environment and thus there is a need for improving the existing methods for the fabrication of carbon materials. As such, this work proposes to discuss, interrogate, and propose viable hydrothermal, solvothermal, and other advanced carbon materials synthesis methods. The synthesis approaches for advanced carbon materials to be interrogated will include the synthesis of carbon dots, carbon nanotubes, nitrogen/titania-doped carbons, graphene quantum dots, and their nanocomposites with solid/polymeric/metal oxide supports. This will be performed with a particular focus on microwave-assisted solvothermal and hydrothermal synthesis due to their favourable properties such as rapidity, low cost, and being green/environmentally friendly. These methods are regarded as important for the current and future synthesis and modification of advanced carbon materials for application in energy, gas separation, sensing, and water treatment. Simultaneously, the work will take cognisance of methods reducing the fabrication costs and environmental impact while enhancing the properties as a direct result of the synthesis methods. As a direct result, the expectation is to impart a significant contribution to the scientific body of work regarding the improvement of the said fabrication methods.
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http://dx.doi.org/10.3390/ma14175094 | DOI Listing |
Chem Commun (Camb)
September 2025
Beijing Advanced Innovation Center for Materials Genome Engineering, Institute for Advanced Materials and Technology, State Key Laboratory for Advanced Metals and Materials, University of Science and Technology Beijing, Beijing 100083, China.
Hard carbon (HC) has emerged as a promising anode material for sodium-ion batteries (SIBs) owing to its low cost, abundant renewable resources, and high specific capacity. However, its practical application is significantly hindered by the severe initial irreversible capacity loss resulting from sodium consumption during the first cycle. To address this issue, a variety of presodiation strategies have been developed to compensate for the sodium loss and improve the initial coulombic efficiency.
View Article and Find Full Text PDFChem Commun (Camb)
September 2025
Key Laboratory of Special Functional Materials for Ecological Environment and Information (Ministry of Education), School of Material Science and Engineering, Hebei University of Technology, Tianjin 300130, P. R. China.
High-performance, low-cost electrocatalysts are essential for freshwater-independent seawater electrolysis. We design a SWCNT-supported (FeCoNiMnCr)O high-entropy spinel oxide by a hydrothermal method and air-firing, where the conductive network enhances charge transfer and active site exposure. The catalyst achieves 282 mV@10 mA cm with 100 h stability in alkaline seawater.
View Article and Find Full Text PDFiScience
September 2025
State Key Laboratory of Advanced Marine Materials, Institute of Oceanology, Chinese Academy of Sciences, Qingdao 266071, China.
Super austenitic stainless steels (SASS) face challenges like galvanic corrosion and antibacterial performance when welded to carbon steel (Q235) in marine environments. This study demonstrates that adding 1.0 wt% cerium (Ce) to SASS refines the heat-affected zone (HAZ) grain structure (from 7 μm to 2 μm), suppresses detrimental σ-phase precipitation, and forms a dense oxide film.
View Article and Find Full Text PDFACS Electrochem
September 2025
Department of Chemistry and Chemical Engineering, Chalmers University of Technology, Kemigården 4, Gothenburg 412 96, Sweden.
Carbon fiber nanotip electrodes (CFNEs) are crucial for electrochemical recordings of neurotransmission release in confined spaces, such as synapses and intracellular measurements. However, fabricating CFNEs with small surface area to minimize noise remains challenging due to inconsistent tip size control, low reproducibility, and low fabrication success rate. Here, we present a reliable, user-friendly method with high reproducibility and success rate for precise CFNE fabrication using microscopy-guided electrochemical etching of cylindrical carbon fiber microelectrodes in a potassium hydroxide droplet.
View Article and Find Full Text PDFACS Electrochem
September 2025
School of Chemistry, University of Nottingham, University Park, Nottingham NG7 2RD, UK.
The study of electrochemical oxidations has wide-ranging implications, from the development of new electrocatalysts for fuel cells for energy conversion, to the synthesis of fine chemicals. 2,2,6,6-Tetramethylpiperidine-1-oxyl (TEMPO) has been used for decades as a sustainable, metal-free mediator for chemical oxidations and is now being used for electrochemical oxidations. We describe here a novel approach to TEMPO-mediated electrooxidations, in which the chemical input and waste generated during electrooxidations of alcohols are minimized by using a multifunctional room temperature ionic liquid (RTIL) to facilitate flow electrosynthesis.
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