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Fiber optic surface plasmon resonance (SPR) sensor utilizing silver (Ag) and Ag-graphene oxide (GO) is designed and developed for the detection of adulteration of glucose and fructose in pure honey. The concentration range of the two adulterants in pure honey is varied from 4% to 20% with a step change of 4%. The experiments were performed with two different fiber optic probes viz. Probe 1 and Probe 2. Probe 1 is fabricated by coating 50 nm Ag film on unclad optical fiber portion and Probe 2 is fabricated by modifying Ag film with GO for sensitivity improvement. The study confirms that using GO modified fiber optic probe, the sensitivity is enhanced to 24% and 37% for glucose and fructose adulterated honey samples respectively. The technique presented in this study is easy, rapid, label free and shows high prospective for the detection of adulterants in pure honey.
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http://dx.doi.org/10.1016/j.foodchem.2020.127346 | DOI Listing |
Food Chem
September 2025
Department of Medical Science, Mahidol University, Amnatcharoen Campus, Amnat Charoen, 37000, Thailand; Department of Chemistry and Center for Innovation in Chemistry, Faculty of Science, Mahidol University, Bangkok, 10400, Thailand. Electronic address:
This study utilized the synergistic effectiveness of chia seed mucilage and iron (III)-natural phenolic nanoparticles as biosorbents for the first time in the dispersive solid-phase extraction (DSPE) of oxytetracycline, tetracycline, chlortetracycline, and doxycycline followed by HPLC-UV quantification. An in-situ iron (III)-natural phenolic solid adsorbent was created using natural phenolics found in the copper pod tree bark. An ultrasonic-assisted extraction was performed to enhance the extraction efficiency of DSPE-based biosorbents.
View Article and Find Full Text PDFTalanta
July 2025
Creative Chemistry and Innovation Research Unit, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science, Mahasarakham University, Maha Sarakham, Thailand; Multidisciplinary Research Unit of Pure and Applied Chemistry (MRUPAC), Department of Chemistry and Cen
The contamination of sulfonamide in food and environmental applications has highlighted a great necessity to develop amphoteric adsorbents for their simultaneous extraction and determination. The combination of cetyltrimethylammonium bromide with alginate-MS, which has a wide surface area, high porosity, high water absorption, and biodegradability, as an adsorbent for the determination of sulfonamide residues by ultra-high performance liquid chromatography-photodiode array detector (UHPLC-PDA) was proposed. Convenient conditions led to the facile synthesis of the sorbent.
View Article and Find Full Text PDFFood Chem
August 2025
Depart. de Ciências Exatas e da Terra, Universidade do Estado da Bahia (UNEB). R. Silveira Martins, 2555, Salvador, Bahia, Brazil. Electronic address:
Food fraud raises significant concerns to consumer health and economic integrity, with the adulteration of honey by sugary syrups representing one of the most prevalent forms of economically motivated adulteration. This study presents a novel framework that combines data from multiple analytical techniques with specialized deep learning models (convolutional neural networks), integrated via meta-learning, in order to differentiate between pure honey and samples adulterated with sugar cane molasses, glucose syrup, or caramel-flavored ice cream topping. Unlike traditional chemometric methods, this approach expands the input feature space, leading to enhanced predictive performance.
View Article and Find Full Text PDFFront Insect Sci
March 2025
College of Food Science and Technology, Yunnan Agricultural University, Kunming, China.
Background: The bacterial diversity of two bee species in the process of honey collection during the flowering season of three different floral sources in the winter was studied. The common bacterium in all samples was .
Methods: In the present study, we collected nectar, honey sacs, and fresh honey during the winter flowering season of , , and .
BMC Complement Med Ther
February 2025
Institute of Molecular Biology, Slovak Academy of Sciences, Dubravska cesta 21, Bratislava, 845 51, Slovakia.
Background: Honey has been successfully used in wound care and cosmetics because of its effective biological properties, including antibacterial, antioxidant, and anti-inflammatory activities. Polyphenols, particularly phenolic acids, are key honey components responsible for these beneficial effects. In recent years, there has been a growing demand for natural, ecologically friendly, and biodegradable products in the modern cosmetics and wound care market.
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