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This study demonstrates a new extraction method for determination of aflatoxins (AFs) in food samples by a GO-SiO/ZnO/FeO nanocomposite as new and effective sorbent. The nanocomposite structure was confirmed by FT-IR, XRD, EDX, FE-SEM, TEM, and mapping techniques. Optimization of the extraction process was conducted by investigating pH, adsorbent amount, sample volume, and solvent volume using central composite design (CCD). The method showed good linearity for AFs B, B, G, and G within specified ranges. Detection and quantification limits were 0.06-0.53 and 0.20-1.62 ng mL, respectively. The high performance liquid chromatography with fluorescence detector assisted by solid phase extraction (SPE-HPLC-FLD) method was applied to food samples, achieving recoveries of 70.15-97.08 %. Accuracy was confirmed through recovery measurements in spiked samples, with ranges of 70.15-97.85 % in wheat, 70.01-91.97 % in chickpeas, and 71.29-93.92 % in white pepper. Reusability and cost-effectiveness suggest its potential for preconcentration and determination of AFs in food samples.
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http://dx.doi.org/10.1016/j.foodchem.2024.142264 | DOI Listing |
JMIR Res Protoc
September 2025
Institute for Collaboration on Health, Intervention, and Policy, University of Connecticut, Storrs, CT, United States.
Background: Children in the United States have poor diet quality, increasing their risk for chronic disease burden later in life. Caregivers' feeding behaviors are a critical factor in shaping lifelong dietary habits. The Strong Families Start at Home/Familias Fuertes Comienzan en Casa (SFSH) was a 6-month, home-based, pilot randomized-controlled feasibility trial that aimed to improve the diet quality of 2-5-year-old children and promote positive parental feeding practices among a predominantly Hispanic/Latine sample.
View Article and Find Full Text PDFJ Am Coll Health
September 2025
Department of Epidemiology and Community Health, College of Health and Human Services, The University of North Carolina at Charlotte, Charlotte, North Carolina, USA.
Despite alarming rates of students' food insecurity in the US (41%), estimates may not be fully capturing experiences in university settings. Understanding students' food insecurity is a knowledge gap flagged amidst outstanding progress on food security measurement in household settings. This study investigated the domains shaping the experiences around food with implications for food insecurity among students.
View Article and Find Full Text PDFCien Saude Colet
August 2025
Programa de Pós-Graduação em Ciência da Nutrição, Departamento de Nutrição e Saúde, Universidade Federal de Viçosa. Av. Peter Henry Rolfs s/n, Campus Universitário. University Campus. 36570-900 Viçosa MG Brasil.
The scope of this study was to characterize the iodine nutritional status of pregnant Brazilian women according to biochemical and dietary markers. It involved a cross-sectional study of 2,376 pregnant women. A semi-structured questionnaire was used to characterize the population.
View Article and Find Full Text PDFSci Adv
September 2025
Department of Bioengineering and Therapeutic Sciences, University of California, San Francisco, San Francisco, CA, USA.
Breastfeeding is essential for reducing infant morbidity and mortality, yet exclusive breastfeeding rates remain low, often because of insufficient milk production. The molecular causes of low milk production are not well understood. Fresh milk samples from 30 lactating individuals, classified by milk production levels across postpartum stages, were analyzed using genomic and microbiome techniques.
View Article and Find Full Text PDFPLoS One
September 2025
Animal Welfare Program, Faculty of Land and Food Systems, The University of British Columbia, Vancouver, British Columbia, Canada.
Non-replacement dairy calves (i.e., males and females not needed for milking herd replacement) can face multiple welfare challenges due to their low economic value in the dairy and beef industries.
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