Nanoindentation of embedded particles.

J Mater Res

Mechanical Metallurgy Laboratory, École Polytechnique Fédérale de Lausanne, MXD 140 (Bâtiment MXD), Station 12, 1015 Lausanne, Switzerland.

Published: February 2023


Category Ranking

98%

Total Visits

921

Avg Visit Duration

2 minutes

Citations

20

Article Abstract

We address the effect of elastic inhomogeneity on elastic modulus and hardness determinations made by depth-sensing indentations performed on individual particles embedded within a matrix of different elastic modulus. Finite element simulations and nanoindentation experiments are used to quantify the consequences of particle/matrix elastic inhomogeneity and we propose an adaptation of the Oliver-Pharr method that gives access to particle properties knowing those of the matrix. The method is suitable for any combination of matrix and particle elastic modulus and for any type of indenter, provided that the area of the tested particles along the surface of the sample is measured and that a large number of particles are probed. Further conditions for the implementation of the method are that testing conditions be such (i) that permanent deformation of the matrix is avoided, and (ii) that permanent deformation in each probed particle under the indenter is not affected by the matrix.

Download full-text PDF

Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC10070221PMC
http://dx.doi.org/10.1557/s43578-023-00920-2DOI Listing

Publication Analysis

Top Keywords

elastic modulus
12
elastic inhomogeneity
8
permanent deformation
8
elastic
5
matrix
5
nanoindentation embedded
4
particles
4
embedded particles
4
particles address
4
address elastic
4

Similar Publications

High-Pressure X‑ray Diffraction Study of Scheelite-Type Perrhenates.

J Phys Chem C Nanomater Interfaces

September 2025

Departamento de Física Aplicada - Instituto de Ciencia de Materiales, Matter at High Pressure (MALTA) Consolider Team, Universidad de Valencia, Edificio de Investigación, C/Dr Moliner 50, 46100 Burjassot, Valencia Spain.

The effects of pressure on the crystal structure of scheelite-type perrhenates were studied using synchrotron powder X-ray diffraction and density-functional theory. At ambient conditions, the studied materials AgReO, KReO, and RbReO, exhibit a tetragonal scheelite-type crystal structure described by space group 4/. Under compression, a transition from scheelite-to-M'-fergusonite (space group 2/) was observed at 1.

View Article and Find Full Text PDF

Background: In catheter-based radiofrequency ablation (RFA), energy is delivered to heterogeneous thin-walled tissues to induce therapeutic heating. Variations in electrical and mechanical properties of tissue contents have a great effect on outcomes.

Purpose: The objective of this study is to develop models that replicate tissue heterogeneity and visualize ablation zones for effective evaluation and optimization.

View Article and Find Full Text PDF

In-situ extrusion 3D printing with tea polyphenol crosslinking for Hyaluronic acid sodium salt -based composite hydrogel scaffolds.

Colloids Surf B Biointerfaces

September 2025

School of Mechanical Engineering, Xinjiang University, Urumqi 830017, PR China; Institute of Bioadditive Manufacturing, Jiangxi University of Science and Technology, Nanchang 330013, PR China.

High-performance hydrogel biomaterials hold considerable promise for advanced wound care. However, the suboptimal mechanical properties of conventional hydrogel materials limit their practical application. In this study, Hyaluronic acid sodium salt (HA), xanthan gum (XG), and N-acryloyl-glycinamide (NAGA) hydrogels with porous structures were successfully fabricated using in-situ extrusion 3D printing technology, and a functionalization strategy involving tea polyphenol (TP) immersion was proposed to enhance material properties through additional hydrogen bonding.

View Article and Find Full Text PDF

Hemostatic intervention at the bleeding site during early-phase wound management plays a crucial role in reducing trauma-induced complications and mortality, while advanced wound dressings facilitate hemorrhage control, exudate management, and antimicrobial protection to promote optimal healing outcomes. To address these issues, we developed a multifunctional collagen/silk fibroin/Mg(OH)₂ (Col/SF/Mg(OH)₂) composite sponge combining enhanced mechanical strength, rapid hemostasis, and broad-spectrum antibacterial activity. The incorporation of silk fibroin (SF) through covalent crosslinking increased the elastic modulus by 4.

View Article and Find Full Text PDF

Programmable self-assembly has recently enabled the creation of complex structures through precise control of the interparticle interactions and the particle geometries. Targeting ever more structurally complex, dynamic, and functional assemblies necessitates going beyond the design of the structure itself, to the measurement and control of the local flexibility of the intersubunit connections and its impact on the collective mechanics of the entire assembly. In this study, we demonstrate a method to infer the mechanical properties of multisubunit assemblies using cryogenic electron microscopy (cryo-EM) and RELION's multi-body refinement.

View Article and Find Full Text PDF