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Progress towards analysing transitions between steady states demands improvements in time-resolved imaging, both for fundamental research and for applications in information technology. Transmission electron microscopy is a powerful technique for investigating the atomic structure, chemical composition and electromagnetic properties of materials with high spatial resolution and precision. However, the extraction of information about dynamic processes in the ps time regime is often not possible without extensive modification to the instrument while requiring careful control of the operation conditions to not compromise the beam quality. Here, we avoid these drawbacks by combining a delay line detector with continuous illumination in a transmission electron microscope. We visualize the gyration of a magnetic vortex core in real space and show that magnetization dynamics up to frequencies of 2.3 GHz can be resolved with down to ∼122ps temporal resolution by studying the interaction of an electron beam with a microwave magnetic field. In the future, this approach promises to provide access to resonant dynamics by combining high spatial resolution with sub-ns temporal resolution.
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http://dx.doi.org/10.1016/j.ultramic.2021.113392 | DOI Listing |
J Am Chem Soc
September 2025
State Key Laboratory of Chemistry for NBC Hazards Protection, College of Chemistry, Fuzhou University, Fuzhou 350116, P. R. China.
The activation of methane and other gaseous hydrocarbons at low temperature remains a substantial challenge for the chemistry community. Here, we report an anaerobic photosystem based on crystalline borocarbonitride (BCN) supported Fe-O nanoclusters, which can selectively functionalize C-H bonds of methane, ethane, and higher alkanes to value-added organic chemicals at 12 °C. Scanning transmission electron microscopy and X-ray absorption spectroscopy corroborated the ultrafine FeOOH and FeO species in Fe-O clusters, which enhanced the interfacial charge transfer/separation of BCN as well as the chemisorption of methane.
View Article and Find Full Text PDFJ Am Chem Soc
September 2025
Department of Chemistry, Boston University, Boston, Massachusetts 02215, United States.
Two-dimensional (2D) materials offer a valuable platform for manipulating and studying chemical reactions at the atomic level, owing to the ease of controlling their microscopic structure at the nanometer scale. While extensive research has been conducted on the structure-dependent chemical activity of 2D materials, the influence of structural transformation during the reaction has remained largely unexplored. In this work, we report the layer-dependent chemical reactivity of MoS during a nitridation atomic substitution reaction and attribute it to the rearrangement of Mo atoms.
View Article and Find Full Text PDFLangmuir
September 2025
School of Light Industry Science and Engineering, Beijing Technology and Business University, Beijing 100048, People's Republic of China.
The study of the self-assembly of surfactants in aqueous solutions, though a traditional field, remains fascinating and full of novelty. In this article, the anionic perfluorodecanoic acid surfactant (PFA) is separately complexed with three hydroxyalkylamines (monoethanolamine (MEA), diethylamine (DEA), and triethanolamine (TEA)) in aqueous solutions. The transformation of aggregate morphologies from spherical unilamellar to nanotubes and then to spherical bilamellar is observed at room temperature, which is confirmed by cryo-transmission electron microscopy (cryo-TEM).
View Article and Find Full Text PDFEnviron Sci Pollut Res Int
September 2025
M. Kumarasamy College of Engineering, Karur, 639113, Tamil Nadu, India.
Energy production from renewable resources remains a leading focus in sustainable power generation. Recently, bifacial photovoltaic (BPV) systems have gained global attention for their enhanced energy yield. In this study, seashell waste was repurposed as an alternative reflector material for BPV modules.
View Article and Find Full Text PDFBiomacromolecules
September 2025
Division of Pharmacy and Optometry, Manchester Institute of Biotechnology, School of Health Sciences, Faculty of Biology, Medicine and Health, The University of Manchester, Oxford Road, M13 9PL Manchester, U.K.
This study investigates how hydrophobic and hydrophilic modifications at the C-terminus of the base peptide, KFEFEFKFK (KbpK), affect the hydrogel macroscopic properties. By the incorporation of phenylalanine (F, hydrophobic) and lysine (K, hydrophilic) residues, four variants, KbpK-K, KbpK-F, KbpK-KF, and KbpK-FK, were designed and evaluated. pH-concentration phase diagrams and Fourier transform infrared confirmed clear links showing how peptide hydrophobicity and charge influence β-sheet formation and macroscopic phase behavior.
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