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Article Abstract
An electrochemical oxidative synthesis of -thiocarbamates by a carbamothioation reaction a three-component coupling reaction (disulfide, water and isocyanide) is developed, which avoids the use of external oxidants and generates only hydrogen gas as the by-product. With NHI as the mediator and electrolyte, the desired -thiocarbamates were obtained in good yields in an undivided cell at room temperature.
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Electrosynthesis of -thiocarbamates with disulfides as a sulfur source.
Chem Commun (Camb)
January 2022
College of Chemistry and Materials Science, Hunan Agricultural University, Changsha, 410128, People's Republic of China.
An electrochemical oxidative synthesis of -thiocarbamates by a carbamothioation reaction a three-component coupling reaction (disulfide, water and isocyanide) is developed, which avoids the use of external oxidants and generates only hydrogen gas as the by-product. With NHI as the mediator and electrolyte, the desired -thiocarbamates were obtained in good yields in an undivided cell at room temperature.
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