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This study portrays a facile wet-chemical synthesis of FeSe/TiO nanocomposites for the first time for advanced asymmetric supercapacitor (SC) energy storage applications. Two different composites were prepared with varying ratios of TiO (90 and 60%, symbolized as KT-1 and KT-2) and their electrochemical properties were investigated to obtain an optimized performance. The electrochemical properties showed excellent energy storage performance owing to faradaic redox reactions from Fe/Fe while TiO due to Ti/Ti with high reversibility.

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