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This study investigates the influence of various drying techniques (freeze drying, vacuum drying, and spray drying) and carrier types (oligofructose, trehalose, palatinose, inulin, and maltodextrin) on the physicochemical properties of elderberry juice powder. The results reveal that freeze drying maintains the highest total polyphenol content (ranging from 0.63 to 1.19 g of gallic acid (GA) per 100 g of dry matter), while spray drying offers practical advantages despite producing lower polyphenol levels. Additionally, the choice of carrier significantly influences the physicochemical properties of the powder, with palatinose yielding results comparable to those obtained through freeze drying. The analysis elucidates the complex relationships between variables, with the two main principal components (PC1 and PC2) explaining 67.21 % of the total variance of the data. This research provides valuable information for the development of elderberry-derived products with improved health-promoting properties.
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http://dx.doi.org/10.1016/j.foodchem.2025.144686 | DOI Listing |
Carbohydr Polym
November 2025
Flavors and Fragrance Engineering & Technology Research Center of Henan Province, College of Tobacco Science, Henan Agricultural University, Zhengzhou 450000, China. Electronic address:
Fragrances are indispensable additives in consumer products including foods, cosmetics, and tobacco products. However, their inherent instability leads to rapid quality degradation and performance loss, driving the urgent need for controlled-release systems to stabilize fragrance performance. In this work, cellulose nanofibers (CNF) were used to prepare CNF aerogel-like gels (CA) and carbonized CNF aerogels (C-CA) through freeze-drying and high-temperature carbonization.
View Article and Find Full Text PDFCarbohydr Polym
November 2025
Institute of Nano and Biopolymeric Materials, School of Materials Science and Engineering, Tongji University, Shanghai 201804, China. Electronic address:
This work reports an ethanol-mediated freeze-drying (EMFD) strategy that enables the scalable production of high-performance bacterial cellulose aerogels (BCAs), effectively addressing key limitations of conventional methods such as supercritical drying and standard freeze-drying, including fragility, low mechanical strength, and high cost. Specifically, by replacing water in bacterial cellulose hydrogels (BCHs) with ethanol-water solution (EWs) prior to freeze-drying, the process limits ice crystal formation and reduces capillary forces and adhesion, thereby preserving structural integrity and enhancing mechanical properties. The effects of EWs concentration on BCA morphology, volume shrinkage, mechanical strength, and pore structure were systematically investigated.
View Article and Find Full Text PDFCritical-sized bone defects present significant clinical challenges due to inadequate vascularization and scaffold integration. This study developed a multifunctional 3D-printed polycaprolactone (PCL)-gelatin (Gel) scaffold reinforced with Bioglass particles (BGPs) or copper dopped BGPs (CuBGPs) to synergistically enhance angiogenesis and bone regeneration in rat model. The scaffolds were fabricated by infiltrating gelatin solutions containing BGPs or CuBGPs into the pores of 3D-printed PCL matrices, followed by freeze-drying.
View Article and Find Full Text PDFInt J Biol Macromol
September 2025
CNR-STIIMA (National Research Council of Italy - Institute of Intelligent Industrial Technologies and Systems for Advanced Manufacturing), Biella, Italy.
A purified-keratin solution obtained from wool fibers by sulfitolysis extraction was employed to produce hydrogels with and without crosslinking. Both hydrogels were used to successfully obtain aerogels by supercritical CO drying. Freeze-dried keratin was also produced from purified keratin solutions as reference materials.
View Article and Find Full Text PDFACS Appl Mater Interfaces
September 2025
Research Center for Materials Nanoarchitectonics, National Institute for Materials Science (NIMS), 1-1 Namiki, Tsukuba 305-0044, Japan.
Sustainable and chemically resilient hydrogels are critically needed in biointerface engineering, particularly for 3D cell culture systems and surface modification under physiological to mildly alkaline conditions. However, physically cross-linked cellulose nanofiber (CNF) hydrogels─despite their renewable origin and biocompatibility─typically disintegrate at pH > 8, limiting their use in polydopamine (PDA)-based surface functionalization. Here, we present a simple and scalable physical treatment strategy to fabricate alkali-resistant, physically cross-linked hydrogels from carboxymethyl cellulose nanofibers (CMCF).
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