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Composite roll produced through casting methods typically remain in the as-cast state after forming. During the preparation process, extended exposure to high temperatures often results in microstructural coarsening at the interface and surface layers, restricting their mechanical performance. To overcome this limitation, we developed a novel vacuum billet forging process for the fabrication of composite rolls. By integrating numerical simulations with experimental validation, we successfully prepared a 42CrMo/Cr5 composite roll. The comprehensive characterization of the interface, including microstructure, elemental distribution, grain texture, grain type, and mechanical properties, was conducted using OM, SEM, EPMA, EBSD, Vickers hardness testing, and a universal testing machine. The relationship between the interface microstructure and mechanical performance was systematically analyzed. The results indicate that complete metallurgical bonding at the interface was achieved with an upsetting reduction ratio of 40% and a single-pass elongation reduction ratio of less than 10%. The interfacial microstructure consisted of four zones: the roll core exhibited lamellar pearlite and blocky ferrite; the diffusion layer near 42CrMo featured pearlite; the diffusion layer near Cr5 contained pearlite and Cr carbides; the Cr5 layer contained fine lamellar pearlite with a greater amount of dispersed Cr carbides. Significant diffusion of Cr and Ni elements was observed, with Cr diffusion extending to 70-90 μm. The interface grains experienced substantial deformation and recrystallization, enhancing the bonding strength. Tensile tests indicated that fracture occurred on the 42CrMo side, with yield and tensile strengths of 371 MPa and 729 MPa, respectively. The microhardness of the composite interface gradually increased from 190 HV to 305 HV without abrupt changes. A significant hardness difference was observed on both sides of the interface, while the variation within the diffusion layer was relatively smooth, indicating good bonding performance at the composite interface.
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http://dx.doi.org/10.3390/ma18010122 | DOI Listing |
JDS Commun
September 2025
Department of Animal Science, Texas A&M University, College Station, TX 77845.
The objectives of this experiment were to evaluate the effects of forage sorghum silage harvest settings, combining cut height, onboard sorghum kernel processor (KP) technology, and ensiling duration, on berry processing score (BPS) and ruminal in situ starch disappearance at 7 h (isSD7). Three harvest settings were tested: a 20-cm cut height, with and without KP (Low+KP, Low-noKP), and a 120-cm cut height with KP (High+KP). A commercial sorghum field was divided into 9 squares, with 3 squares randomly selected as blocks.
View Article and Find Full Text PDFACS Omega
September 2025
Department of Physics, Birla Institute of Technology and Science, Pilani, Pilani Campus, Vidya Vihar, Pilani, Rajasthan 333031, India.
We report the performance of solid-state ceramic supercapacitors (SSCs) based on a novel composite electrolyte comprising aluminum-doped lithium lanthanum titanate perovskite, LiLaTiAlO (Al-doped LLTO), and the ionic liquid 1-ethyl-3-methylimidazolium tetrafluoroborate (EMIM BF). Rietveld refinement of X-ray diffraction data confirms the preservation of the tetragonal perovskite phase after Al substitution, indicating structural stability of the host lattice. X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy further corroborate the successful incorporation of Al without forming secondary phases.
View Article and Find Full Text PDFThe functionalization of thin, flexible glass with piezoelectric oxides is a pathway toward transparent electromechanical devices. The crystallization of lead zirconate titanate thin films on thick, rigid glass is previously demonstrated using flash lamp annealing to selectively anneal the films, without damaging the substrates. In this work, a 2-step process suitable for Schott AF 32 eco glass and Corning Willow glass is developed, both 100 μm thick, the latter of which is compatible with roll-to-roll processes.
View Article and Find Full Text PDFSensors (Basel)
August 2025
Institute of Management and Technology, Hochschule Osnabrück, Kaiserstr. 10c, 49809 Lingen, Germany.
This work focuses on time and frequency domain analyses of IMU-based orientation estimation algorithms, including indirect Kalman (IKF), Madgwick (MF), and complementary (CF) filters. Euler angles and quaternions are used for orientation representation. A 6-DoF IMU is attached to a 6-joint UR5e robotic arm, with the robot's orientation serving as the reference.
View Article and Find Full Text PDFPolymers (Basel)
August 2025
Division of Polymer Engineering and Rubber Industrial Technology, Department of Mechanical Engineering Technology, College of Industrial Technology, King Mongkut's University of Technology North Bangkok, Bangkok 10800, Thailand.
This study investigated the development of biocomposites for use as packaging and film in everyday applications. The utilization of rice flour (RF) as a cheap natural filler in the production of polybutylene succinate (PBS) biocomposites has been shown to reduce environmental issues caused by non-biodegradable plastic waste. The effect of rice flour content on the morphology and properties of PBS and RF biocomposites was comprehensively evaluated.
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